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Y/MCM-41复合分子筛的合成及表征

田莎 李会鹏 赵华 齐相前 韩聪 董海进 宋国

石油化工高等学校学报Issue(6):20-24,5.
石油化工高等学校学报Issue(6):20-24,5.DOI:10.3969/j.issn.1006-396X.2015.06.004

Y/MCM-41复合分子筛的合成及表征

Synthesis and Characterization of Y/MCM-41 Composite Molecular Sieve

田莎 1李会鹏 1赵华 1齐相前 1韩聪 1董海进 1宋国2

作者信息

  • 1. 辽宁石油化工大学化学化工与环境学部,辽宁抚顺 113001
  • 2. 抚顺石化公司石油二厂,辽宁抚顺 113000
  • 折叠

摘要

Abstract

The Y/MCM-41 composite molecular sieve was prepared by post-synthesis method and its performance was characterized by XRD,BET,N2 adsorption-desorption and so on.In addition,its hydrothermal stability was studied.The results showed that the optimized synthesis conditions are as follows:pH 1 1,CTAB and SiO 2 molar ratio of 0.1 5,crystallization time 48 h,and the composite molecular sieve had the properties of both mesoporous MCM-41 and microporous Y.The acidity and hydrothermal stability of composite molecular sieve were better than that of pure mesoporous MCM-41.

关键词

复合分子筛 Y/MCM-41/合成/表征/酸度/水热稳定性

Key words

Y/MCM-41composite molecular sieve/Synthesis/Characterization/Acidity/Hydrothermal stability

分类

能源科技

引用本文复制引用

田莎,李会鹏,赵华,齐相前,韩聪,董海进,宋国..Y/MCM-41复合分子筛的合成及表征[J].石油化工高等学校学报,2015,(6):20-24,5.

基金项目

大学生创新训练计划项目国家级甲等(201410148008) (201410148008)

辽宁省自然科学基金项目(2014020109)。 (2014020109)

石油化工高等学校学报

OACSTPCD

1006-396X

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