中国医药科学Issue(20)：201-203,3.
滴定法测定保婴散中朱砂（HgS）的含量
Titrimetric determination of cinnabar(HgS) content in baoying powders
黄轩 1黄灿林 2谢雪葵 1吕鸯鸯1
作者信息
- 1. 广东省肇庆市第二人民医院药剂科，广东肇庆526040
- 2. 广东一力集团制药有限公司，广东四会526200
- 折叠
摘要
Abstract
ObjectiveTo establish the methods of titrimetric determination of cinnabar (HgS) content in baoying powders.MethodsTo make the corresponding determination adopted the chemical titration with the digestants of sulphuric acid and potassium nitrate, the titration solution of ammonium rhodanate. At the same time, to make interrelated experiment such as dried in the shade test, replicate test, average recovery test and so on.Results The sampling amount was 1.2g as there was no significant difference with shorter time of digestion, less consumption of titration solution compared with the sampling amount of 2.4g and 4.8g. Under the sampling amount of 1.2g, the cinnabar(HgS) content in baoying powders had better repeatability ofRSD=0.58%(n=6) with the average recovery of 98.96%, RSD=0.55%.Conclusion Titrimetric determination of cinnabar(HgS) content in baoying powders has the characteristic of simple operation, reliable, accurate and so on, could be used on quality control of this kind of preparation.关键词
滴定法/保婴散/朱砂/含量测定Key words
Titration/Baoying powders/Cinnabar/Determination分类
医药卫生引用本文复制引用
黄轩,黄灿林,谢雪葵,吕鸯鸯..滴定法测定保婴散中朱砂（HgS）的含量[J].中国医药科学,2015,(20):201-203,3.
