印染助剂2015，Vol.32Issue(12)：48-52,5.
高效液相色谱法测定纺织品中的邻苯二甲酸酯
Determination of phthalate in textiles by high performance liquid chromatography
摘要
Abstract
The determination of ten kinds of phthalate (PAEs) by high performance liquid chromatography (HPLC) was developed. After extracted from textiles by fat instrument with ether, PAEs was eluted from C18 stationery liquid column with gradient elution of acetonitrile and water, and detected by diode- array detector (DAD). The detection wavelength was 225 nm, column temperature was 35 ℃, the injection volume was 10μL, the flow rate was 1.2 mL/min. The recovery rate was 98.4%~101% and precision of relative standard devi-ation (RSD) values was 2.9%~5.3%, both of which met the technical requirements of residue analysis.关键词
邻苯二甲酸酯/高效液相色谱/纺织品/测定Key words
phthalate (PAEs)/high performance liquid chromatography (HPLC)/textile/determination分类
化学工程引用本文复制引用
周佳,潘生林,丁友超,郭亚飞,曹锡忠,钱凯..高效液相色谱法测定纺织品中的邻苯二甲酸酯[J].印染助剂,2015,32(12):48-52,5.基金项目
国家质量监督检验检疫总局科研项目(2013IK107) （2013IK107）
江苏出入境检验检疫局科研课题(2012KJ20) （2012KJ20）
