核化学与放射化学Issue(6):435-440,6.DOI:10.7538/hhx.2015.37.06.0435
模拟放射性污染土壤样品中147 Pm 的分离及液闪测量
Separation and Liquid Scintillation Analysis of 147 Pm in Radioactive Polluted Soil Sample
马越 1刘志超 1张丽莉 1张继红1
作者信息
- 1. 西北核技术研究所,陕西 西安 710024
- 折叠
摘要
Abstract
Focused on the environmental soil sample contaminated by spent fuel,a Pm sepa-ration procedure was established with a recovery greater than 70% for Pm and the decontam-ination factor greater than 10 3 for the interference elements.The activity of 1 47 Pm standard sample was determined by liquid scintillation counting (LSC)with the efficiency tracing method (ETM),giving a relative deviation less than 0.5%.The analysis method of 1 47 Pm was validated for simulated polluted soil sample (prepared by mixing the spent fuel with environmental soil)and the results are in good agreement with the referenced data with a relative deviation of 2%.关键词
147Pm/147Nd/液闪测量/效率示踪Key words
147Pm/147Nd/liquid scintillation counting/efficiency tracing method分类
化学化工引用本文复制引用
马越,刘志超,张丽莉,张继红..模拟放射性污染土壤样品中147 Pm 的分离及液闪测量[J].核化学与放射化学,2015,(6):435-440,6.