天津中医药Issue(2)：107-110,4.DOI:10.11656/j.issn.1672-1519.2016.02.12
血府逐瘀方不同制剂中挥发性成分的GC-MS 分析
Identification of the volatile components in different preparations of Xuefu Zhuyu by GC-MS
摘要
Abstract
Objective] To identify the volatile components in different preparations of Xuefu Zhuyu, a rapid GC-MS method was established. [Methods] Headspace gas chromatography-mass spectrometry (HS-GC/MS) was employed for identification of the components in Xuefu Zhuyu capsules, Xuefu Zhuyu soft capsules, Xuefu Zhuyu tablets and Xuefu Zhuyu oral liquid. The volatile components were retrieved by NIST-10 library, the relative percentage contents of which were calculated by area normalization method. [Results] The 21 volatile components were identified from Xuefu Zhuyu capsules, including acetic acid, benzaldehyde, ligustilide and 2-methyl-butanal etc. The 22 volatile components were identified in Xuefu Zhuyu tablets, including limonene, 3-methyl-butanal, ligustilide and 2-methyl-butanal etc. Ten and five volatile components were identified in Xuefu Zhuyu soft capsules and Xuefu Zhuyu oral liquid, respectively.[Conclusion] In this study, the method established can be used for the detection and analysis of volatile components in different preparation of Xuefu Zhuyu. The results could provide the basis for the quality control of preparation of Xuefu Zhuyu.关键词
顶空气相色谱-质谱联用法/血府逐瘀方/挥发性成分Key words
pace gas chromatography-mass spectrometry/Xuefu Zhuyu preparation/volatile component分类
医药卫生引用本文复制引用
于卉娟,杨帆,江振作,王跃飞,杨欣莹..血府逐瘀方不同制剂中挥发性成分的GC-MS 分析[J].天津中医药,2016,(2):107-110,4.基金项目
国家自然科学基金资助项目（81202877）。 （）
