中国药房2016，Vol.27Issue(3)：392-394,3.DOI:10.6039/j.issn.1001-0408.2016.03.36
柴葛感冒合剂的质量标准研究
Study on the Quality Standard for Chaige Ganmao Mixture
陈倩倩 1孙洪胜2
作者信息
- 1. 山东中医药大学药学院,济南 250035
- 2. 山东中医药大学附属医院,济南 250011
- 折叠
摘要
Abstract
OBJECTIVE:To establish the quality standard for Chaige ganmao mixture. METHODS:TLC was conducted to iden-tify the Scutellaria baicalensis and Paeonia lactiflora;HPLC was conducted to determine the content of puerarin. The column was Zorbax Eclipse XDB-C18 with mobile phase of methanol-water(25:75,V/V)at flow rate of 1.0 ml/min,detection wavelength was 250 nm,and column temperature was 25℃,and the injection volume was 5μl. RESULTS:TLC showed clear spots and good sepa-ration. The linear range of puerarin was 18-198 μg/ml(r=0.999 9);RSDs of precision,stability and reproducibility tests were low-er than 2%,recovery was 99.04%-99.75%(RSD=0.28%,n=6). CONCLUSIONS:The standard can be used for the quality con-trol of Chaige ganmao mixture.关键词
柴葛感冒合剂/质量标准/薄层色谱法/高效液相色谱法/黄芩/白芍/葛根素Key words
Chaige ganmao mixture/Quality standard/TLC/HPLC/Scutellaria baicalensis/Paeonia lactiflora/Puerarin分类
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陈倩倩,孙洪胜..柴葛感冒合剂的质量标准研究[J].中国药房,2016,27(3):392-394,3.
