化工进展Issue(2):544-548,5.DOI:10.16085/j.issn.1000-6613.2016.02.031
磷酸/草酸混合溶液中锥形多孔阳极氧化铝的制备和表征
Fabrication and characterazation of anodic alumina with tapered porous structure
摘要
Abstract
A method to fabricate highly ordered tapered porous anodic alumina (PAA) templates in mixed solution which contains phosphoric acid and oxalic acid was presented. Firstly,highly ordered PAA templates with interpore distance of 495nm were fabricated by two-step method. On this basis, ordered tapered PAA templates with different aspect ratios were fabricated by alternately performing anodization process and pore widening process. Results showed that the aspect ratio of tapered PAA templates is linearly related to the total anodizing time,which could reach more than 100. And the relationship between tapered PAA morphology and partial anodizing time/partial pore widening time was also discussed in detail. The special structure of nano-template could expand the applications of PAA templates in fabricating metal or semiconductor nanowires,photoelectric materials and polymer materials.关键词
多孔阳极氧化铝/锥形结构/多层纳米结构Key words
porous anodic alumina/tapered structure/multi-layer nanostructure分类
化学化工引用本文复制引用
徐艳芳,李晓久,刘皓..磷酸/草酸混合溶液中锥形多孔阳极氧化铝的制备和表征[J].化工进展,2016,(2):544-548,5.基金项目
国家自然科学基金面上项目(51473122)、国家大学生创新训练计划(201510058034)及天津市高等学校科技发展基金计划(20120321)项目。 ()