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高品质碳酸镧晶簇的合成与表征

宋金凤 张玉倩

药学研究2016,Vol.35Issue(3):154-156,3.
药学研究2016,Vol.35Issue(3):154-156,3.DOI:10.13506/j.cnki.jpr.2016.03.010

高品质碳酸镧晶簇的合成与表征

Synthesis and characterization of high medicinal value lanthanum carbonate with a layer -crystal structure

宋金凤 1张玉倩1

作者信息

  • 1. 青岛普瑞森医药科技有限公司,山东 青岛 266111
  • 折叠

摘要

Abstract

Objective To synthesize high medicinal value lanthanum carbonate,and characterize the synthetic sim-ples.Methods Lanthanum carbonate was synthesized by lanthanum chloride and sodium bicarbonate.It can be synthesized by changing synthesis conditions,which include adjusting pH value and adding different additives.Furthermore,the synthet-ic samples were characterized by several techniques including X -ray diffraction (XRD),Fourier transform infrared spec-trometer (FTIR),scanning electron microscopy (SEM),and Thermo gravimetric analyzer (TGA).Results The results showed that layer -crystal was synthesized by adding ethanol in the synthetic systems,and the crytal size was 20 ~50 μm with a layer up to 0.6 ~0.8 μm thick.Conlusion The higher specific surface area of lanthanum carbonate was more fa-vorable to the combination of phosphate,and can reduce the absorption of phosphorus in the gastrointestinal tract.

关键词

碳酸镧/晶簇/有机溶剂

Key words

Lanthanum carbonate/Layer -crystal/Ethanol

分类

药学

引用本文复制引用

宋金凤,张玉倩..高品质碳酸镧晶簇的合成与表征[J].药学研究,2016,35(3):154-156,3.

药学研究

2095-5375

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