药学研究2016,Vol.35Issue(3):154-156,3.DOI:10.13506/j.cnki.jpr.2016.03.010
高品质碳酸镧晶簇的合成与表征
Synthesis and characterization of high medicinal value lanthanum carbonate with a layer -crystal structure
宋金凤 1张玉倩1
作者信息
- 1. 青岛普瑞森医药科技有限公司,山东 青岛 266111
- 折叠
摘要
Abstract
Objective To synthesize high medicinal value lanthanum carbonate,and characterize the synthetic sim-ples.Methods Lanthanum carbonate was synthesized by lanthanum chloride and sodium bicarbonate.It can be synthesized by changing synthesis conditions,which include adjusting pH value and adding different additives.Furthermore,the synthet-ic samples were characterized by several techniques including X -ray diffraction (XRD),Fourier transform infrared spec-trometer (FTIR),scanning electron microscopy (SEM),and Thermo gravimetric analyzer (TGA).Results The results showed that layer -crystal was synthesized by adding ethanol in the synthetic systems,and the crytal size was 20 ~50 μm with a layer up to 0.6 ~0.8 μm thick.Conlusion The higher specific surface area of lanthanum carbonate was more fa-vorable to the combination of phosphate,and can reduce the absorption of phosphorus in the gastrointestinal tract.关键词
碳酸镧/晶簇/有机溶剂Key words
Lanthanum carbonate/Layer -crystal/Ethanol分类
药学引用本文复制引用
宋金凤,张玉倩..高品质碳酸镧晶簇的合成与表征[J].药学研究,2016,35(3):154-156,3.