化工进展2016，Vol.35Issue(4)：1149-1153,5.DOI:10.16085/j.issn.1000-6613.2016.04.029
不同制备方法对纳米氢氧化镁性能的影响
Effect of different preparation methods on the properties of magnesium hydroxide nanoparticles
摘要
Abstract
Magnesium hydroxide nanoparticles were prepared via ordinal precipitation method,reverse precipitation method,double precipitation method and high-gravity precipitation method using magnesium chloride hexahydrate as raw material and sodium hydroxide as precipitant. The settling velocity was selected as the index to investigate the effects of different preparation methods on the settlement property of magnesium hydroxide slurry. The morphology,particle size and its distribution, and crystal phase of the samples were characterized by transmission electron microscope (TEM),laser particle size analyzer (LPSA),and X-ray diffractometer (XRD),respectively. The results showed that the settling velocity increased evidentlyvia high-gravity precipitation method,which was 4.7 times, 12.4 times and 2.1 times of that by the ordinal precipitation method,reverse precipitation method and double precipitation method. It was also found that the samples prepared by high-gravity precipitation method were hexagonal flake-like shape with narrow particle size distribution,high purity and good dispersity.关键词
液相沉淀法/超重力/沉降/氢氧化镁/浆料Key words
liquid precipitation method/high gravity/sedimentation/magnesium hydroxide/slurry分类
化学化工引用本文复制引用
申红艳,刘有智,马鹏程,索奇,刘雪莉,彭云鹏,朱芝敏..不同制备方法对纳米氢氧化镁性能的影响[J].化工进展,2016,35(4):1149-1153,5.基金项目
国家自然科学基金项目（21376229）。 （）
