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丹芩消郁合剂质量标准研究

蒋洁莹 刘瑾 李世芳 沈婷婷

四川中医2016,Vol.34Issue(3):103-106,4.
四川中医2016,Vol.34Issue(3):103-106,4.

丹芩消郁合剂质量标准研究

Study on Quality Standard of Danqinxiaoyu Mixture

蒋洁莹 1刘瑾 1李世芳 1沈婷婷1

作者信息

  • 1. 上海中医药大学附属曙光医院药剂科,上海200021
  • 折叠

摘要

Abstract

Objective To establish the quality control method of Danqinxiaoyu Mixture,provide the basis for control the product quality.Methods Radix Scutellariae,Radix paeoniae alba in Danqinxiaoyu Mixture were qualitative identified by TLC;the HPLC method was adopted to determine the baicalin content.Results Radix Scutellariae,Radix paeoniae alba,Radix Angelicae Sinensis in Danqinxiaoyu Mixture could be detected by TLC;the sample size of baicalin within the concentration range of 0.0188mg/ml ~ 1.2mg/ml had good linear relationship with the peak area (R2 =0.9994);the average recovery rate was 100.3%,RSD=1.7%.Conclusion:The established method is strongly specific,accurate and simple,and can better control the quality of Danqinxiaoyu Mixture.

关键词

丹芩消郁合剂/黄芩苷/薄层鉴别法/高效液相色谱法

Key words

Danqinxiaoyu Mixture/baicalin/TLC/HPLC

分类

医药卫生

引用本文复制引用

蒋洁莹,刘瑾,李世芳,沈婷婷..丹芩消郁合剂质量标准研究[J].四川中医,2016,34(3):103-106,4.

基金项目

上海市科委项目-医院制剂的质量标准再提高和稳定性研究(编号:11DZ1972901). (编号:11DZ1972901)

四川中医

OACSTPCD

1000-3649

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