四川中医2016,Vol.34Issue(3):103-106,4.
丹芩消郁合剂质量标准研究
Study on Quality Standard of Danqinxiaoyu Mixture
摘要
Abstract
Objective To establish the quality control method of Danqinxiaoyu Mixture,provide the basis for control the product quality.Methods Radix Scutellariae,Radix paeoniae alba in Danqinxiaoyu Mixture were qualitative identified by TLC;the HPLC method was adopted to determine the baicalin content.Results Radix Scutellariae,Radix paeoniae alba,Radix Angelicae Sinensis in Danqinxiaoyu Mixture could be detected by TLC;the sample size of baicalin within the concentration range of 0.0188mg/ml ~ 1.2mg/ml had good linear relationship with the peak area (R2 =0.9994);the average recovery rate was 100.3%,RSD=1.7%.Conclusion:The established method is strongly specific,accurate and simple,and can better control the quality of Danqinxiaoyu Mixture.关键词
丹芩消郁合剂/黄芩苷/薄层鉴别法/高效液相色谱法Key words
Danqinxiaoyu Mixture/baicalin/TLC/HPLC分类
医药卫生引用本文复制引用
蒋洁莹,刘瑾,李世芳,沈婷婷..丹芩消郁合剂质量标准研究[J].四川中医,2016,34(3):103-106,4.基金项目
上海市科委项目-医院制剂的质量标准再提高和稳定性研究(编号:11DZ1972901). (编号:11DZ1972901)