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高效液相色谱法测定骨刺片中柚皮苷含量

汪秀月

中国药业2016,Vol.25Issue(4):77-78,2.
中国药业2016,Vol.25Issue(4):77-78,2.

高效液相色谱法测定骨刺片中柚皮苷含量

Content Determination of Naringin in Guci Tablets by HPLC

汪秀月1

作者信息

  • 1. 安徽省阜阳市食品药品检验检测中心,安徽 阜阳 236015
  • 折叠

摘要

Abstract

Objective To establish an HPLC method for the content determination of naringin in Guci Tablets. Methods The chro-matographic column was Waters Fire C18 column (250 mm × 4. 6 mm,5 μm),the mobile phase was acetonitrile-water(20 : 80),the detection wavelength was 283 nm,the flow rate was 1. 0 mL/min,the column temperature was 30 ℃. Results The linear relation was good when the injection volume of naringin was in the range of 0. 280 32-2. 803 2 μg( r=1. 000 0,n=5). The average recovery rate was 99. 15%,and RSD was 1. 65%( n=9). Conclusion This method is simple,rapid,has good repeatability,high sensitivity and is reliable,which can be used for the content determination of naringin in Guci Tablets.

关键词

骨刺片/高效液相色谱法/柚皮苷

Key words

Guci Tablets/HPLC/naringin

分类

中医学

引用本文复制引用

汪秀月..高效液相色谱法测定骨刺片中柚皮苷含量[J].中国药业,2016,25(4):77-78,2.

中国药业

OACSTPCD

1006-4931

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