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混合氯化石蜡中短链氯化石蜡定量分析方法的比较

幸苑娜 冯岸红 叶淋泉 林志惠 陈茜 陈泽勇

色谱2016,Vol.34Issue(3):346-350,5.
色谱2016,Vol.34Issue(3):346-350,5.DOI:10.3724/SP.J.1123.2015.10022

混合氯化石蜡中短链氯化石蜡定量分析方法的比较

Comparison of quantitative analytical methods of short chain chlorinated paraffins in chlorinated paraffin mixtures

幸苑娜 1冯岸红 1叶淋泉 1林志惠 1陈茜 1陈泽勇1

作者信息

  • 1. 深圳市计量质量检测研究院,广东 深圳 518131
  • 折叠

摘要

Abstract

Total response factor correction method and multiple linear regression method were adopted to quantify the sum of short chain chlorinated paraffins( SCCPs)in chlorinated paraffin mixtures. Both methods were based on electron capture negative ionization mass spectrometry. The results showed that high SCCPs quantitative accuracies were obtained by the two methods both with eliminating the potential interferences of mediumchain chlorinated paraffins. However,both two methods were slightly dependent on the ranges of calibration solutions. Dilution of the sample solution was necessary when performing these two methods. Besides, multiple linear regression method was suitable for more wide-quantitative-range of SCCPs than total response factor correction method.

关键词

总体响应因子校正法/多元线性回归法/短链氯化石蜡

Key words

total response factor correction method/multiple linear regression method/short chain chlorinated paraffins(SCCPs)

分类

化学化工

引用本文复制引用

幸苑娜,冯岸红,叶淋泉,林志惠,陈茜,陈泽勇..混合氯化石蜡中短链氯化石蜡定量分析方法的比较[J].色谱,2016,34(3):346-350,5.

基金项目

广东省质量技术监督局科技项目(2013PJ03)@@@@Technology Project of Administration of Quality and Technology Supervision of Guangdong Province( No.2013PJ03). ()

色谱

OA北大核心CSCDCSTPCDMEDLINE

1000-8713

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