云南化工2016,Vol.43Issue(2):13-16,4.DOI:10.3969/j.issn.1004-275X.2016.02.004
乙烯基硅烷偶联剂改性白炭黑
Research on Modification of Silica by Vinyl Silica Coupling Agent
摘要
Abstract
Vinyl silane coupling agent as modifier,selection the appropriate temperature for hydroly-sis,precipitated silica surface was modified.Effects of dosage of modifier,temperature,time on the modifica-tion were discussed.The optimal conditions for the surface modification by orthogonal experiment were con-cluded as using vinyl triethoxy as modifier,with every 10.00 g silica modifier dosage of 4.00 g,the modifica-tion time for 30 minutes,modification temperature of 70 ℃.Under such conditions,the modified product acti-vation degree could be reached more than 95%.The infrared spectrum analysis showed that there was chemi-cally bonding formation between hydrolyzed vinyl silane coupling agent and silica surface.关键词
沉淀白炭黑/表面改性/乙烯基硅烷偶联剂/水解Key words
precipitated silica/surface modification/vinyl silane coupling agent/hydrolysis分类
化学化工引用本文复制引用
裴莹,苟继贤,李佳奇,黄斌..乙烯基硅烷偶联剂改性白炭黑[J].云南化工,2016,43(2):13-16,4.基金项目
四川省大学生创新创业训练计划(201410622014)。 ()