药学研究2016，Vol.35Issue(4)：202-204,3.DOI:10.13506/j.cnki.jpr.2016.04.004
香附中mesocyperusphenol A的含量测定研究
Study on determination of mesocyperusphenol A in fruit of Cyperus rotundus L.
摘要
Abstract
Objective To establish an UHPLC method for the determination of mesocyperusphenol A in fruit of Cyperus rotundus L. ,and provide a quality control method for Cyperus rotundus L. . Methods The chromatography was carried out on a Poroshell 120 EC - C18 column(3. 0 mm × 150 mm,1. 8 μm)with acetonitrile - water(28∶72,V∶V)as the mobile phase,the detection wavelength was 325 nm. Results Mesocyperusphenol A could be successfully determined and the line-ar rang was 0. 784 ~ 7. 84 μg·mL - 1(r = 0. 999 7). The average recovery of mesocyperusphenol A was 101. 6% ,RSD =1. 39%(n = 6). The content of mesocyperusphenol A in 6 batches was 3. 72 ~ 10. 00 μg·g - 1 . Conclusion Mesocyperus-phenol A was the specific ingredient in fruit of Cyperus rotundus L. . The method was accurate,reliable and sensitive for the quality control of fruit of Cyperus rotundus L. .关键词
香附/Mesocyperusphenol A/超高效液相色谱/含量测定Key words
Cyperus rotundus L./Mesocyperusphenol A/UHPLC/Determination分类
医药卫生引用本文复制引用
邓仕任,朱夏敏,王鑫,朱江,夏林波..香附中mesocyperusphenol A的含量测定研究[J].药学研究,2016,35(4):202-204,3.基金项目
国家自然科学基金项目（ No.81202857）；辽宁省高等学校优秀人才支持计划（ No. LJQ2015070）；辽宁省自然科学基金 （）
