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生胃颗粒的质量标准研究

谭梅英 孙冬梅 李智勇

按摩与康复医学2016,Vol.7Issue(16):49-52,53,5.
按摩与康复医学2016,Vol.7Issue(16):49-52,53,5.

生胃颗粒的质量标准研究

Study on the Quality Standard of Shengwei Granules

谭梅英 1孙冬梅 2李智勇2

作者信息

  • 1. 广东省第二中医院,广东广州510095
  • 2. 广东省中医药工程技术研究院,广东广州510095
  • 折叠

摘要

Abstract

Objective:To establish the quality controlling and analyzing method for Shengwei granules. Methods:Thin-layer chromatography (TLC) was used to identify the astragalus membranaceus, pseudo-ginseng, bupleurum and fructus aurantii that contained in Shengwei granules, and used high performance liquid chromatography (HPLC) to test the content of astragaloside. Results:The thin-layer chromatography (TLC) that established in this study can effectively identify the astragalus membranaceus, pseudo-ginseng, bupleurum and fructus aurantii, which spots were clear and nega-tive samples had no interference;the astragaloside presented a good linear relationship in the range of 2.014~10.070μg (r=0.9994), the average recov-ery rate was 97.31%, RSD=1.08%. Conclusion:The TLC and HPLC that established in this study are simple operating, rapid, high accuracy, and the specificity are good, so can be used in quality control of Shengwei granules.

关键词

生胃颗粒/黄芪甲苷/薄层色谱法/高效液相色谱法/质量控制

Key words

Shengwei granules/astragaloside/thin-layer chromatography (TLC)/high performance liquid chromatography/quality control

分类

医药卫生

引用本文复制引用

谭梅英,孙冬梅,李智勇..生胃颗粒的质量标准研究[J].按摩与康复医学,2016,7(16):49-52,53,5.

基金项目

广东省中医药管理局资助课题--生胃颗粒的研究与开发,编号20161017 ()

按摩与康复医学

1008-1879

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