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烈味脚骨脆的化学成分研究

季飞飞 康静 谢春锋 许婧 郭远强

药学研究2016,Vol.35Issue(6):311-314,4.
药学研究2016,Vol.35Issue(6):311-314,4.DOI:10.13506/j.cnki.jpr.2016.06.001

烈味脚骨脆的化学成分研究

Studies on the chemical constituents of Casearia graveolens

季飞飞 1康静 2谢春锋 1许婧 2郭远强3

作者信息

  • 1. 哈尔滨商业大学药学院,黑龙江 哈尔滨 150076
  • 2. 南开大学药学院,天津 300071
  • 3. 南开大学药学院,天津 300071
  • 折叠

摘要

Abstract

Objective To study the chemical constituents of Casearia graveolens.Methods The chemical constituents were isolated and purified through silica gel column chromatograph and HPLC.The structures of isolated compounds were e-lucidated on the basis of spectroscopic methods.Results Seven compounds were isolated and identified asbalanspene B (1 ),balanspene E(2),rel -(2S,5R,8S,9S,1 0R,1 8S,1 9R)-1 8,1 9 -diacetoxy -1 8,1 9 -epoxy -2 -(2 ξ-methylbu-tanoyloxy)cleroda -3,1 3(1 6),1 4 -triene(3),balanspene G(4),caseabalansin G(5),caseabalansin F(6),caseamem-brin U (7).Conclusion Compounds 1 ~7 were isolated from Casearia graveolens for the first time.

关键词

烈味脚骨脆/大风子科/化学成分/二萜

Key words

Casearia graveolens/Flacouritaecac/Chemical constituents/Diterpenoids

分类

医药卫生

引用本文复制引用

季飞飞,康静,谢春锋,许婧,郭远强..烈味脚骨脆的化学成分研究[J].药学研究,2016,35(6):311-314,4.

基金项目

国家自然科学基金(No.21372125);天津市自然科学基金(No.13JCQNJC13600);高等学校博士学科点专项科研基金资助课题 ()

药学研究

2095-5375

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