中国药业2016，Vol.25Issue(8)：16-19,4.
消炎散质量控制研究
Quality Control of Xiaoyan Powders
摘要
Abstract
Objective To establish the quality control method of Xiaoyan Powders. Methods Xiaoyan Powders was identified by TLC and the contents of emodin and chrysophanold were determined by HPLC. Results TLC spots were clear. Emodin and Chrysophanold had a good linear relationship among 0. 018 6-0. 127 6 μg( r=0. 999 6)and 0. 041 0-0. 406 0 μg( r=1. 000 0)respectively. The average recovery rate of emodin and chrysophanold were 100. 37 % and 91. 41%,the RSD were 3. 57% and 1. 95% ( n=6). Conclusion The qualitative identification is accurate,the HPLC method is accurate and specific with good reproducibility. It can be used for quantity control of Xiaoyan Powders.关键词
大黄素/大黄酚/消炎散/高效液相色谱法/薄层色谱法/质量控制Key words
emodin/chrysophanold/Xiaoyan Powders/HPLC/TLC/quality control分类
医药卫生引用本文复制引用
蓝献丽,巫玲玲,蓝彬,植国繁,罗春水,蒋敏捷,蒋伟哲,孔晓龙..消炎散质量控制研究[J].中国药业,2016,25(8):16-19,4.基金项目
广西壮族自治区西南特色民族药物开发工程研究中心项目，项目编号桂教科研[2013]8号－3。 （）
