中国药业2016，Vol.25Issue(10)：72-73,2.
超高效液相色谱－质谱联用法检测不同品种龟甲制龟甲胶的牛皮源成分
Identification of Bovine-Hide Gelatin from Glue of Tortoise Shell Made by Different Kinds of Tortoise Shell by UPLC-MS
彭婷婷 1江勋1
作者信息
- 1. 湖南省衡阳市食品药品检验检测中心，湖南 衡阳 421001
- 折叠
摘要
Abstract
Objective To investigate the influence of using different kinds of tortoise shell on the content of bovine-hide gelatin from glue of tortoise shell. Methods The UPLC-MS method was performed on the Zorbax C18 column (50 mm × 2. 1 mm,1. 8 μm),by a gradient elution using 0. 1% formic acid aqueous solution-0. 1% formic acid in acetonitrile as the mobile phase at a flow rate of 0. 3 mL/min and at 40 ℃. Glue of tortoise shell were detected which were made from different kinds of tortoise shell. Results It was founded that the test results were positive which contained Trachemys scripta eleganns shell,while negative results were detected which were made by pure Chinemys reevesiis shell. Conclusion The method is simple,accucate,specific and high sensitivity which provided a basis for quality′s effective control of glue of tortoise shell.关键词
超高效液相色谱-质谱联用法/龟甲/龟甲胶/牛皮源成分Key words
UPLC-MS/tortoise shell/glue of tortoise shell/bovine-hide gelatin分类
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彭婷婷,江勋..超高效液相色谱－质谱联用法检测不同品种龟甲制龟甲胶的牛皮源成分[J].中国药业,2016,25(10):72-73,2.
