中南大学学报（自然科学版）2016，Vol.47Issue(5)：1494-1499,6.DOI:10.11817/j.issn.1672-7207.2016.05.006
In2O3-10SnO2陶瓷中In4Sn3O12与富Sn析出相特征
Characteristics of In4Sn3O12and Sn-rich precipitate in In2O3-10SnO2 ceramic
摘要
Abstract
ITO ceramics were prepared using co-precipitation powders which contained 10% SnO2.The samples were sintered at 1600℃for different time in oxygen atmosphere. The phase composition, element distribution and microstructure of ceramics were studied by XRD, EPMA, TEM and SEM. The results show that nanosized Sn-rich phase with body-centered cubic structure precipitatesin In2O3:Sn grains. Meanwhile, In4Sn3O12grains form at triple junctions of In2O3:Sn grains, and precipitate-free zones appear around In2O3:Sn grain boundaries. The sizes and distancesof Sn-rich precipitates in In2O3:Sn grains decrease gradually from grain center to grain boundary. Furthermore, the sizes of In4Sn3O12grains and Sn-rich precipitates as well as the width of precipitate-free zones increase with extension of the holding time.关键词
ITO陶瓷/In4Sn3O12晶粒/富Sn析出相/微观结构Key words
ITO ceramic target/In4Sn3O12grains/Sn-rich precipitate/microstructure分类
信息技术与安全科学引用本文复制引用
侯俊峰,周科朝,李志友,王科,甘雪萍..In2O3-10SnO2陶瓷中In4Sn3O12与富Sn析出相特征[J].中南大学学报（自然科学版）,2016,47(5):1494-1499,6.基金项目
湖南省科技计划项目(2014GK2011)(Project(2014GK2011)@@@@supported byHunan Science and Technology Plan) （2014GK2011）
