日用化学工业2016，Vol.46Issue(5)：302-304,3.DOI:10.13218/j.cnki.csdc.2016.05.013
气相色谱法检测湿巾中丙二醇的含量
Determination of propylene glycol content in wet wipes by gas chromatography
摘要
Abstract
A weighted sample of wet wipe was extracted by ethanol under assistance of ultrasonic wave,and the extract was filtered via centrifugation. Then the filtrate was detected by gas chromatography to determine the content of propylene glycol in wet wipes. The quantification was identified with external standard method. Results showed that the method exhibits good linearity in the mass concentration range of 2.50-200.00 mg/L. For 1,2-propylene glycol,the correlation coefficient is 0.998 9,detection limit is 1.50 mg/L,RSDA=2.32%, and spiked recovery is 92.10% -97.20%. For 1,3-propylene glycol,the correlation coefficient is 0.999 4, detection limit is 2.00 mg/L,RSDA=3.15%,and spiked recovery is 93.40% -97.25%.关键词
湿巾/丙二醇/气相色谱法Key words
wet wipes/propylene glycol/gas chromatography分类
化学化工引用本文复制引用
成霈,杨悦,靳尧..气相色谱法检测湿巾中丙二醇的含量[J].日用化学工业,2016,46(5):302-304,3.基金项目
国家质量监督检验检疫总局科技计划资助项目 （）
