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怀地黄中地黄苷D的提取工艺及不同炮制品含量的比较研究

张彩 张萍 司文琪 赵燕 史磊

山东农业科学2016,Vol.48Issue(5):127-130,4.
山东农业科学2016,Vol.48Issue(5):127-130,4.DOI:10.14083/j.issn.1001-4942.2016.05.023

怀地黄中地黄苷D的提取工艺及不同炮制品含量的比较研究

Study on Extraction Process of Rehmannioside D in Radix Rehmanniae and Its Content Comparison in Different Processed Products

张彩 1张萍 1司文琪 1赵燕 1史磊1

作者信息

  • 1. 山东中医药大学药学院,山东 济南 250355
  • 折叠

摘要

Abstract

To establish the extraction process of rehmannioside D in Radx Rehmanniae,and compare its content in different processed products,the single factor experiments were conducted to optimize the extraction process,and the HPLC method was adopted to detect the rehmannioside D content.The results showed that the optimal extraction conditions were heating reflux extraction for 2 hours with 60% of methanol,which was stable and reliable with higher extraction rate.The content of rehmannioside D in Radix Rehmanniae was 0.250%,which was higher than that in Radix Rehmanniae Praeparata (0.208%).

关键词

怀地黄/地黄苷D/高效液相色谱

Key words

Radix Rehmanniae/Rehmannioside D/High performance liquid chromatography (HPLC)

分类

农业科技

引用本文复制引用

张彩,张萍,司文琪,赵燕,史磊..怀地黄中地黄苷D的提取工艺及不同炮制品含量的比较研究[J].山东农业科学,2016,48(5):127-130,4.

基金项目

山东中医药大学2015年度大学生研究训练计划(SRT)项目 ()

山东农业科学

OACSTPCD

1001-4942

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