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卷烟侧流烟气中氨释放量的连续流动法测定

王洪波 郭军伟 殷延齐 刘绍锋 赵晓东 谢复炜 赵乐

烟草科技2016,Vol.49Issue(5):38-44,7.
烟草科技2016,Vol.49Issue(5):38-44,7.DOI:10.16135/j.issn1002-0861.20160506

卷烟侧流烟气中氨释放量的连续流动法测定

Determination of ammonia in sidestream cigarette smoke by continuous flow analysis method

王洪波 1郭军伟 1殷延齐 2刘绍锋 1赵晓东 1谢复炜 1赵乐1

作者信息

  • 1. 中国烟草总公司郑州烟草研究院,郑州高新技术产业开发区枫杨街2号 450001
  • 2. 江苏中烟工业有限责任公司徐州卷烟厂,江苏省徐州市环城路80号 221000
  • 折叠

摘要

Abstract

An analytical method for quantifying ammonia in sidestream cigarette smoke (SCS) was developed with continuous flow analysis. Ammonia in SCS was collected by a“fishtail”chimney, by passing through a Cambridge filter pad and an absorption bottle containing hydrochloric acid. The combined collection was subjected to washing and extraction before being analyzed by a continuous flow method. The results showed that: 1)The method had good linearity (with correlation coefficient of 0.999 9)and the limit of detection was 0.12 mg/cig. The relative standard deviation was 6.8% (n=5), and the recoveries ranged from 86.0% to 112.0%. 2)The method was simple, rapid, accurate, and suitable for determining the level of ammonia in SCS.

关键词

卷烟/侧流烟气//连续流动法

Key words

Cigarette/Sidestream smoke/Ammonia/Continuous flow analysis

分类

轻工纺织

引用本文复制引用

王洪波,郭军伟,殷延齐,刘绍锋,赵晓东,谢复炜,赵乐..卷烟侧流烟气中氨释放量的连续流动法测定[J].烟草科技,2016,49(5):38-44,7.

基金项目

中国烟草总公司标准预研项目“卷烟侧流烟气中氨的测定”(2014QB012)。 ()

烟草科技

OA北大核心CSCDCSTPCD

1002-0861

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