中国现代中药2016,Vol.18Issue(5):591-594,4.DOI:10.13313/j.issn.1673-4890.2016.5.011
畲药搁公扭根的质量标准研究
Study on Quality Standard of Traditional She Medicine "Ge gongniugen"
摘要
Abstract
Objective:To improve the quality standard of traditional she medicine—Ge gongniugen.Methods:The microscopical characteristics were identified by microscopical method,and index ingredient (Gallic acid)were determined by HPLC.The water content,total ash and ethanol-soluble extractives were determined according to the method in appendix of"pharmacopoeia of people’s republic of china".Results:Characteristics of microscopical identification of Ge gongniugen were obviously.A good linearity of psoralen was at 3.881 ~38.81 μg·mL -1 (r =0.999 7),and the average recovery rate was 99.47% (n =6),RSD =1.22%.The content of gallic acid in 14 batches of Ge gongniugen was in the range of 0.28%-1.46%.The results of water content,total ash and ethanol-soluble extractives were in the range of 5.0%-10.2%,1.4%-3.6% and 14.4%-41.8%,respectively.Conclusion:This method is simple,accurate,applicable for the quality control of Ge gongniugen.关键词
畲药/搁公扭根/质量标准/没食子酸/高效液相色谱法Key words
Traditional She medicine/Ge gongniugen/quality standard/gallic acid/HPLC引用本文复制引用
王伟影,毛菊华..畲药搁公扭根的质量标准研究[J].中国现代中药,2016,18(5):591-594,4.基金项目
[基金项目]丽水市科技局项目(2012CXTD09-05);丽水市科技局项目(2012CXTD11-03);丽水市科技局项目 ()