现代农业科技Issue(7)：293-296,4.
液相色谱-串联质谱法测定大菱鲆中硝基呋喃类代谢物的不确定度评定
Uncertainty Evaluation for Determination of Nitrofuran Metabolites in Turbot by High Performance Liquid Chromatography-Tandem Mass Spectrometry
摘要
Abstract
According to Ministry of Agriculture Bulletin 783 - 1 -2006, an uncertainty evaluation was established for evaluating the determination results of nitrofuran metabolites in turbot by high performance liquid chromatography-tandem mass spectrometry.According to the mathematical model , the uncertainty components were analyzed,quantified and composed,which included standard curve fitting,repeat measurement of samples,the preparation of standard solution , the weight of samples , the constant volume of samples.By the results , the residues of AOZ , SEM , AHD and AMOZ in turbot were 4.17μg/kg,4.48μg/kg,4.25μg/kg,4.45μg/kg,and the expanded uncertainty were 0.24μg/kg,0.23μg/kg,0.24μg/kg,0.23μg/kg(k=2), respectively.关键词
大菱鲆/硝基呋喃类代谢物/不确定度/液相色谱-串联质谱法/测定Key words
turbot/nitrofuran metabolites/uncertainty/high performance liquid chromatography-tandem mass spectrometry/determination分类
化学化工引用本文复制引用
邢丽红,付树林,孙晓杰,郭江涛,孙伟红..液相色谱-串联质谱法测定大菱鲆中硝基呋喃类代谢物的不确定度评定[J].现代农业科技,2015,(7):293-296,4.基金项目
2014年国家水产品质量安全风险评估项目(GJFP2014009). （GJFP2014009）
