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两种纯化工艺对大黄水提液中蒽醌类成分的影响研究

张驰 夏新华 周莉莉 李朝 周宇

湖南中医药大学学报2016,Vol.36Issue(8):30-33,4.
湖南中医药大学学报2016,Vol.36Issue(8):30-33,4.DOI:10.3969/j.issn.1674-070X.2016.08.008

两种纯化工艺对大黄水提液中蒽醌类成分的影响研究

Influences of Two Purification Processe on Anthraquinones in Aqueous Extract Solution of Rheum palmatum

张驰 1夏新华 1周莉莉 1李朝 1周宇1

作者信息

  • 1. 湖南中医药大学药学院,湖南 长沙 410208
  • 折叠

摘要

Abstract

Objective To explore the effect laws of chitosan flocculation clarification and alcohol precipitation process on the anthraquinones in aqueous extract solution of Rheum palmatum. Methods The retention rates of five anthraquinones in Rheum palmatum are as evalution indexes, the influences of two purification processes under the different conditions on the anthraquinones were investigated. Results Under the different conditions of two purification processes, the retention rates of five anthraquinones in aqueous extract solution of Rheum palmatum almost had the same laws: rhein > aloe emodin > emodin >chrysophanol >emodin methyl ether. Comparing two purification processes, the retention rates of alcohol precipitation process on anthraquinones were superior to ones of chitosan flocculation clarification process. Conclution The retention rates of low polarity constituents by alcohol precipitation were better than the chitosan flocculation clarification process, while the high polarity constituents were opposite.

关键词

大黄/蒽醌类/壳聚糖/絮凝澄清/醇沉

Key words

Rheum palmatum/anthraquinones/chitosan/flocculation clarification/alcohol precipitation

分类

医药卫生

引用本文复制引用

张驰,夏新华,周莉莉,李朝,周宇..两种纯化工艺对大黄水提液中蒽醌类成分的影响研究[J].湖南中医药大学学报,2016,36(8):30-33,4.

基金项目

国家自然科学基金面上项目(30973955)。 ()

湖南中医药大学学报

OACSTPCD

1674-070X

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