安徽农业科学2016，Vol.44Issue(18)：45-48,4.
高效液相色谱－质谱联用技术测定土壤中PAEs
Determination of PAEs in Soil by HPLC-MS/MS
摘要
Abstract
Objective] The aim was to determine 22-PAEs in soil samples and establish detection and evaluation method.[Method] By using HPLC-MS/MS method, 22-PAEs were determined with multi reaction monitoring scanning mode.[Result] Detection of samples at the level of 0.50 to 2.00 mg/kg, 22 kinds of PAEs compounds in the detection of mass concentration range:0.10-3.00 mg/L with a good linear rela-tionship, the correlation coefficient r >0.990 0, the linear equation was obtained; recovery rate was 80.20%-139.50%, detection limit was 0.000 1-0.050 0 mg/kg.[Conclusion] HPLC-MS/MS detection method for PAEs compounds is established, which is suitable for resi-due analysis of PAEs compounds in soil.关键词
土壤/塑化剂(PAEs)/HPLC-MS/MSKey words
Soil/Phthalate Acid Ester (PAEs)/HPLC-MS/MS分类
农业科技引用本文复制引用
杨秀娟,吴静娜,王运儒,杜国冬,农耀京..高效液相色谱－质谱联用技术测定土壤中PAEs[J].安徽农业科学,2016,44(18):45-48,4.基金项目
广西热作所科研业务费专项项目（桂热研201501）。 （）
