吡虫啉在烟草中的残留分析及调制对其残留的影响OA北大核心CSCDCSTPCD
Analysis of imidacloprid residue and influences of curing methods on its residue in flue-cured and air-cured tobacco
为了解吡虫啉在烟草中的残留行为及调制对该药残留的影响，采用乙腈作为提取液、N-丙基乙二胺(PSA)等作为净化吸附剂，建立了吡虫啉在烟叶中残留量的快速样品前处理（QuEChERS）-HPLC检测方法。结果表明：①该法的最低检出限为0.02 mg/kg，以0.1、0.5、1.0 mg/kg吡虫啉的添加量分别添加到烟叶空白样品中，回收率为88.6%~96.6%，变异系数为2.05%~3.42%。②当药剂使用量为4 mg(a.i)/株时，吡虫啉对一般刺吸…查看全部>>
In order to study the imidacloprid residue and the influences of curing methods on its residue in tobacco, a method was developed for determining the imidacloprid residues in tobacco by QuEChERS-HPLC. A pre-treatment approach known as QuEChERS was followed: leaf samples were extracted with acetonitrile, and cleaned up with N-propyl ethylenediamine sorbent before analysis by HPLC. The results showed that: 1) The detection limit(LOD)of imidacloprid was 0.02 mg…查看全部>>
刘丽;何正川;白建保;周敏;程新胜
中国科学技术大学烟草与健康研究中心，合肥市徽州大道1129号 230052四川省宣汉县烟草公司，四川省宣汉县东乡镇西街86号 636150中国烟草总公司职工进修学院，郑州市金水区鑫苑路7号 450008安徽皖南烟叶有限责任公司芜湖经理部，安徽省芜湖县湾址环城南路 241100中国科学技术大学烟草与健康研究中心，合肥市徽州大道1129号 230052
农业科技
吡虫啉烤烟白肋烟残留调制方法
ImidaclopridFlue-cured tobaccoBurley tobaccoResidueCuring method
《烟草科技》 2016 (8)
64-69,6
河南省烟草公司科技项目“烟粉虱防治的关键技术研究与示范”（20130011）。
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