中国现代中药2016,Vol.18Issue(7):913-915,941,4.DOI:10.13313/j.issn.1673-4890.2016.7.024
龙胆泻肝片质量标准研究
Quality Standard for Longdan Xiegan Tablets
张红玉 1胡松谋 1刘剑 1王继陈1
作者信息
- 1. 云南云河药业股份有限公司,云南 个旧 661000
- 折叠
摘要
Abstract
Objective: To establish a quality standard for Longdan Xiegan Tablets.Methods: Microscopic identification was used by qualitative identification of Gentiana scabra Bge and Scutellaria baicalensis Georgi;TLC was used for qualitative identification of G.scabra and Gardenia jasminoides Ellis;HPLC was used for the determination of gentiopicrin of G.scabra.Results:Microscopic identification showed obvious characteristics,TLC spots were clear;the linear ranges of gentiopicrin was 0.104 8 ~0.628 8 μg (r >0.999).Rate of recovery was 100.4%(n =6).Conclusion:The method is accurate reliable and reproducible and can be used for quality control of Longdan Xiegan Tablets.关键词
龙胆泻肝片/显微鉴别/薄层色谱/高效液相色谱/龙胆苦苷/栀子苷Key words
Longdan Xiegan Tablets/microscopic identification/TLC/HPLC/gentiopicrin/geniposide引用本文复制引用
张红玉,胡松谋,刘剑,王继陈..龙胆泻肝片质量标准研究[J].中国现代中药,2016,18(7):913-915,941,4.