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微萃取-聚结分离技术在碳四脱甲醇中的应用

刘森 杨强 张学清 苗志强

化工进展2016,Vol.35Issue(8):2609-2614,6.
化工进展2016,Vol.35Issue(8):2609-2614,6.DOI:10.16085/j.issn.1000-6613.2016.08.49

微萃取-聚结分离技术在碳四脱甲醇中的应用

Removal of methanol in carbon four by microextraction-colescence separation technology

刘森 1杨强 1张学清 2苗志强2

作者信息

  • 1. 华东理工大学化学工程联合国家实验室,上海 200237
  • 2. 寿光市联盟石油化工有限公司,山东寿光 262700
  • 折叠

摘要

Abstract

To solve the limitations of methanol washing tower efficiency and the problem of excessive amounts of methanol content in the mixed carbon four in a mixed carbon four deep processing project in a petrochemical company,a complete sets of technical equipment of a hybrid micro extraction coupled modular depth of coalescence separation is developed for removal of methanol in the carbon four. The pilot test is performed at a side line of the petrochemical company. The experimental results show that at the inlet and outlet pressure drop of 5kPa,water injection 5%,retention time within 180s and the inlet methanol content of 300—400μL/L,1200—1400μL/L and 40000—50000μL/L in the mixed carbon four,the outlet methanol content is 10—30μL/L,50—100μL/L and 4000—5000μL/L with a separation efficiency higher than 96%,95% and 88%,respectively. The features of deep and quick separation ability of methanol with low pressure drop at a wider range of elasticity of operation show that the technology has a good applicability in the system of water elution of methanol in carbon four,providing a new way of separating the mixed carbon four and methanol.

关键词

碳四/微萃取/聚结分离/甲醇

Key words

carbon four/micro-extraction/coalescence separation/methanol

分类

化学化工

引用本文复制引用

刘森,杨强,张学清,苗志强..微萃取-聚结分离技术在碳四脱甲醇中的应用[J].化工进展,2016,35(8):2609-2614,6.

基金项目

国家自然科学基金项目(51208200)、基本科研业务费交叉学科与重大项目培育基金(222201313001)及上海市晨光计划(13CG26)。 ()

化工进展

OA北大核心CSCDCSTPCD

1000-6613

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