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用中心切割气相色谱法测定车用汽油中甲缩醛及苯胺类化合物含量研究

张利萍 杜娟 闫江

中国标准化Issue(8):84-87,4.
中国标准化Issue(8):84-87,4.DOI:10.3969/j.issn.1002-5944.2016.08.011

用中心切割气相色谱法测定车用汽油中甲缩醛及苯胺类化合物含量研究

Research on the Determination of Methylal and Aniline Compounds Content in Motor Gasoline by Heart-Cut Gas Chromatography

张利萍 1杜娟 1闫江2

作者信息

  • 1. 内蒙古石油化工监督检验研究院
  • 2. 北京超越未来科技发展有限公司
  • 折叠

摘要

Abstract

An external standard method for determination of illegal additives in gasoline by heart-cut gas chromatography is developed in this paper to rapidly analyze methylal and aniline compounds. Results show that, the linear relation of seven target compounds is good in the range of 0~30% (V/V). The recoveries of the additives are in the range of 95.37%~103.10%. The relative standard deviations of six repeated determinations are less than 2.00%. The study shows that the detection limit of methylal is 0.00134%, and the detection limits of aniline compounds are less than 0.002%.

关键词

车用汽油/气相色谱法/甲缩醛/苯胺类化合物

Key words

gasoline/gas chromatography/methylal/aniline compound

引用本文复制引用

张利萍,杜娟,闫江..用中心切割气相色谱法测定车用汽油中甲缩醛及苯胺类化合物含量研究[J].中国标准化,2016,(8):84-87,4.

中国标准化

OACHSSCD

1002-5944

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