山东中医杂志2016，Vol.35Issue(8)：736-738,753,4.
山东道地药材丹参脂溶性成分指纹图谱及多指标成分同时定量研究
Study on Fingerprint and Simultaneous Determination of Multi-components of Lipid-soluble Components of Genuine Salvia miltiorrhiza Bunge in Shandong Province
摘要
Abstract
Objective:To establish the fingerprint of lipid-soluble components of genuine salvia miltiorrhiza bunge in Shandong and to perform simultaneous determination of three components in it.Methods:The analysis were performed on Sciences-InertSustain C18 column,with acetonitrile-0.02％ phosphoric acid solution as the eluent.The flow rate was 1.0 mL/min and the temperature was 30 ℃.Results:Twenty common peaks were identified form the fingerprints of 10 batches of salvia miltiorrhiza bunge and the similarities were not less than 0.940.The linear ranges of tanshinone Ⅰ,tanshinoneⅡ A and cryptotanshinone were 0.11～2.2 μg,0.052～1.04 μg and 0.043～0.086.Conclusion:The established method is simple and the result was accurate.They can provide reference for quality control of salvia miltiorrhiza bunge.关键词
丹参/脂溶性成分/指纹图谱/多指标成分/定量分析Key words
salvia miltiorrhiza bunge/lipid-soluble components/fingerprint/multi-components/quantitative analysis分类
医药卫生引用本文复制引用
窦锦明,王振华,徐楠,荆汉卫..山东道地药材丹参脂溶性成分指纹图谱及多指标成分同时定量研究[J].山东中医杂志,2016,35(8):736-738,753,4.基金项目
潍坊市中医药科研立项项目(2015年第一类编号006号) （2015年第一类编号006号）
