安徽农业科学2016，Vol.44Issue(24)：131-135,5.
D101大孔树脂富集白术内酯Ⅰ和III工艺研究
Technology of Atractylenolide Enrichment I and III by D101 Macroporous Resin
摘要
Abstract
Abst ract [Objective] To research the enrichment process of atractylconolideⅠand III with Atracttylodes macrocephala Koidz as the research materials.[ Method] The enrichment effects of 6 different macroporous resins were compared by static adsorption and desorption experiments.Dy-namic test was carried out on the best macroporous resin.[Result]The optimal technology of atractylconolide Ⅰand III enrichment by D101 macroporous resin was as follows:mass concentrations of atractylcnolideⅠand III were 25.6.2 and 59.7 μg/mL,respectively;4 BV sample vol-ume,2 BV/h flow rate,eluting with 16 BV water,6 BV 30% ethanol and 12 BV 75% ethanol in turn .Under this condition,the the recovery rate of atractylcnolideⅠand III were up to 100.00% and 98.24%,respectively.[Conclusion] It is a simple and effective enrichment process of atrac-tylcnolide from crude extracts of Atracttylodes macrocephala Koidz by D101 macroporous.关键词
白术/白术内酯/富集/大孔树脂/工艺条件Key words
Atracttylodes macrocephala Koidz/Atractylenolide/Enrichment/Macroporous resin/Technology condition分类
医药卫生引用本文复制引用
周玫,梁志远,甘秀海,冉晓燕,何军..D101大孔树脂富集白术内酯Ⅰ和III工艺研究[J].安徽农业科学,2016,44(24):131-135,5.基金项目
贵阳市乌当区科学技术计划项目（［2012］乌科技合同字第53号）。 （）
