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绵萆薢化学成分的分离与结构鉴定

晁利平 阮静雅 刘艳霞 韩立峰 王涛 张祎

天津中医药大学学报2016,Vol.35Issue(5):336-339,4.
天津中医药大学学报2016,Vol.35Issue(5):336-339,4.DOI:10.11656/j.issn.1673-9043.2016.05.13

绵萆薢化学成分的分离与结构鉴定

Isolation and structural identification of constituents from Dioscoreae spongiosae Rhizoma

晁利平 1阮静雅 1刘艳霞 1韩立峰 1王涛 1张祎1

作者信息

  • 1. 天津市中药化学与分析重点实验室,天津 300193
  • 折叠

摘要

Abstract

Objective] Study on chemical constituents of Dioscoreae spongiosae Rhizoma. [Methods] The chemical constituents were obtained by ODS, Sephadex LH-20 and PHPLC chromatorgraphy isolation, and identified by chemical and spectral analysis. [Results] The structures of seven comounds were elucidated to be tachioside (1), isotachioside (2), koaburaside (3), 2,6-dimethoxy-4-hydroxyphenol-1-O-β-D-glucopyranoside (4), icariside D2 ( 5 ) , benzyl alcohol O-β-D-glucopyranoside ( 6 ) , and adenosine ( 7 ) , respectively . [ Conclusion ] Compounds 1~3 were obtained from Dioscoreae genus firstly, and 4~7 was isolated from the plant for the first time.

关键词

绵萆薢/化学成分/结构鉴定

Key words

Dioscoreae spongiosae Rhizoma/chemical constituents/structural identification

分类

医药卫生

引用本文复制引用

晁利平,阮静雅,刘艳霞,韩立峰,王涛,张祎..绵萆薢化学成分的分离与结构鉴定[J].天津中医药大学学报,2016,35(5):336-339,4.

基金项目

新世纪优秀人才支持计划资助项目(NCET-12-1069);天津市高等学校创新团队培养计划资助项目(TD12-5033)。 ()

天津中医药大学学报

OACSTPCD

1673-9043

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