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生物质基固体材料中生物基含量测定方法的研究进展

邓坤明 王鹏飞 马艳 王宏晓 沈娟章 谭卫红

生物质化学工程2016,Vol.50Issue(5):53-59,7.
生物质化学工程2016,Vol.50Issue(5):53-59,7.DOI:10.3969/j.issn.1673-5854.2016.05.010

生物质基固体材料中生物基含量测定方法的研究进展

Research P rogress of Determination Method of Bio-based Content in Bio-based Solid Material

邓坤明 1王鹏飞 1马艳 1王宏晓 1沈娟章 1谭卫红1

作者信息

  • 1. 中国林业科学研究院 林产化学工业研究所 生物质化学利用国家工程实验室国家林业局 林产化学工程重点开放性实验室 江苏省 生物质能源与材料重点实验室,江苏 南京 210042
  • 折叠

摘要

Abstract

The determination methods of bio-based content in bio-based solid material,including the selective dissolution method (SDM) and 14C method,were reviewed.The precision of SDM was relatively lower,and its sample preparation was more complex and time consuming.14C method contained liquid scintillation counting(LSC) method,which included CO2 absorption method, direct LSC method and benzene synthesis,and accelerator mass spectrometry(AMS) method.CO2 absorption method was simple, fast and low cost,but it was also low precision. This method was suitable for the sample requirement for not high precision. The sample preparation of direct LSC method was the simplest in all methods, but it had a high requirement on the samples. This method had a lot of interference factors which were difficult to be eliminated.Benzene synthesis method had high precision,but the sample pretreatment took time,and the measuring period was long. Accelerator mass spectrometry was a rapid detection method and also had high precision,but the equipment was extremely expensive.These all limited its application.Finally,the prospects for their future development were also presented.

关键词

固体材料/生物基含量/选择性溶解法/14C法

Key words

solid material/bio-based content/selective dissolution/14C method

分类

化学化工

引用本文复制引用

邓坤明,王鹏飞,马艳,王宏晓,沈娟章,谭卫红..生物质基固体材料中生物基含量测定方法的研究进展[J].生物质化学工程,2016,50(5):53-59,7.

基金项目

公益性行业科研专项(2012104006-5) (2012104006-5)

江苏省大型科学仪器设备共享服务平台分析测试技术及方法研究课题(无编号) (无编号)

生物质化学工程

OA北大核心

1673-5854

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