材料工程2016，Vol.44Issue(11)：96-100,5.DOI:10.11868/j.issn.1001-4381.2016.11.016
g-C3N4／NiO复合材料的制备及其对AP热分解的影响
Preparation of g-C3 N4/NiO Composites and Its Effect on T hermal Decomposition of Ammonium Perchlorate
摘要
Abstract
g‐C3 N4/NiO composites were prepared by a simple mixing‐calcination method .The struc‐ture and morphology of g‐C3N4/NiO were characterized by X‐ray Diffraction(XRD) ,Fourier Trans‐form Infrared Spectrometer (FT‐IR) ,Field Emission Scanning Electron Microscopy (FESEM ) and En‐ergy Dispersive X‐ray spectroscopy(EDS) .The catalytic effect of g‐C3N4/NiO on thermal decomposi‐tion of ammonium perchlorate (AP) was investigated by Differential Thermal Analysis (DTA ) and Thermo Gravimetric Analysis (TG) .The results show that nanometer NiO is uniformly dispersed on the surface of g‐C3 N4 ,g‐C3 N4/NiO composites make the two decomposition peaks of AP combine and the high‐temperature decomposition peak value of AP decrease by 62 .5℃ ,which exhibits good cata‐lytic performance .The catalytic activity of g‐C3 N4/NiO is much higher than that of single‐phase g‐C3 N4 and NiO ,clearly demonstrating a synergistic effect between g‐C3 N4 and NiO .关键词
g-C3 N4/NiO/高氯酸铵/催化性能/热分解/协同作用Key words
g-C3 N4/NiO/ammonium perchlorate/catalysis/thermal decomposition/synergistic effect分类
通用工业技术引用本文复制引用
谈玲华,徐建华,寇波,杭祖圣,石丽丽,王钧..g-C3N4／NiO复合材料的制备及其对AP热分解的影响[J].材料工程,2016,44(11):96-100,5.基金项目
江苏省自然科学基金（BK20130747）；江苏省高校自然科学研究课题（14KJD430002）；江苏省先进结构材料与应用技术重点实验室开放基金（ASMA201408）；南京工程学院校级科研基金项目 （）
