中国药业2016，Vol.25Issue(22)：67-68,2.
高效液相色谱法测定巴戟口服液中淫羊藿苷含量
Content Determination of Icariin in Baji Oral Liquid by HPLC
潘伟 1赵悦 1王小柳1
作者信息
- 1. 重庆市永川食品药品检验所，重庆 402160
- 折叠
摘要
Abstract
Objective To establish an HPLC method for the content determination of icariin in Baji Oral Liquid. Methods The Syncro-nis C18 column(250 mm × 4. 6 mm,5 μm)was used with a mobile phase consisting of CH3CN-H2O(30 :70)at the flow rate of 1. 0 mL/min;the column temperature was maintained at 30 ℃,and the detection wavelength was set at 270 nm. Results The standard curve for icariin was linear in the range of 0. 010 2-0. 101 5 μg. The average recovery was 99. 38% with RSD of 1. 51%( n=6). Conclusion The method is simple,accurate,reproducible,and can be used to the quality control of Baji Oral Liquid.关键词
巴戟口服液/高效液相色谱法/淫羊藿苷/含量测定Key words
Baji Oral Liquid/HPLC/icariin/content determination分类
医药卫生引用本文复制引用
潘伟,赵悦,王小柳..高效液相色谱法测定巴戟口服液中淫羊藿苷含量[J].中国药业,2016,25(22):67-68,2.
