郑州大学学报(工学版)2016,Vol.37Issue(6):10-14,5.DOI:10.13705/j.issn.1671-6833.2016.03.022
水热法合成微纳米CuO及在气体传感器中的应用
Hydrothermal Synthesis of CuO Micro/Nanoparticles and Their Application in Gas Sensors
摘要
Abstract
Micro/Nano-particles of CuO were prepared with hexamethylenetetramine template. The composi-tion and morphology of the product were characterized by SEM and X-ray diffraction. The synthetic powder was prepared as sensitive membrane, and its gas sensitivity was studied with a static gas distribution method. The results indicated that the uniform copper oxide powders was synthesized at the 110℃, and the molar ratio be-tween copper nitrate and hexamethylenetetramine was 1∶45. The spindle structure was around 1~2 μm, and was composed of 100 nm nanoplates. The sensor had better selectivity with CH3 COCH3 and H2 S. Copper ox-ide showed good selectivity to hydrogen sulfide and its sensitivity had a certain degree of improvement after fur-ther doping 0. 25% ~1. 25% noble metal catalyst Pt.关键词
气体传感器/氧化铜颗粒/水热法/掺杂Key words
gas sensor/copper oxide particles/hydrothermal method/doping分类
化学化工引用本文复制引用
胡校兵,谢祯芳,谢骥,解丽丽,朱志刚..水热法合成微纳米CuO及在气体传感器中的应用[J].郑州大学学报(工学版),2016,37(6):10-14,5.基金项目
国家自然科学基金资助项目(61471233) (61471233)
上海高校特聘教授(东方学者)计划 (东方学者)
上海市科委基础研究重点项目(13NM1401300) (13NM1401300)
上海市教委曙光计划项目(14SG52) (14SG52)
上海市人才基金资助项目(201346) (201346)