安徽农业科学2016，Vol.44Issue(33)：83-85,115,4.
电感耦合等离子体质谱法测定大米中几种重金属元素含量
Determination of Several Heavy Metals Content in Rice by Inductively Coupled Plasma Mass Spectrometry
卢伦 1赵凯 1吴晓芳 1徐坚琪 1沈群1
作者信息
- 1. 杭州市质量技术监督检测院，浙江杭州310019
- 折叠
摘要
Abstract
Objective] The aim was to determine several heavy metals content in rice rapidly and accurately, to provide reference for research on heavy metal pollution in rice.[Method] The content of lead, arsenic, cadmium, mercury, chromium, copper, zinc and selenium in rice were determined by inductively coupled plasma mass spectrometry (ICP-MS) with microwave digestion.The conditions for the determination of 8 ele-ments were optimized.[Result] The results showed that the correlation coefficient of 8 elements in rice is greater than 0.999 6 in the linear range, the detection limit is 0.18 -20.00 μg/kg, the recovery rate is 91.6%-106.0%, the relative standard deviation is 0.5%-9.7%. [Conclusion] The method is simple, sensitive and accurate.It is suitable for the detection of the content of lead, arsenic, cadmium, mercury, chromium, copper, zinc and selenium in rice.关键词
大米/电感耦合等离子体质谱法/重金属Key words
Rice/Inductively coupled plasma mass spectrometry/Heavy metal分类
轻工纺织引用本文复制引用
卢伦,赵凯,吴晓芳,徐坚琪,沈群..电感耦合等离子体质谱法测定大米中几种重金属元素含量[J].安徽农业科学,2016,44(33):83-85,115,4.
