日用化学品科学2016，Vol.39Issue(11)：21-25,5.DOI:10.13222/j.cnki.dc.2016.11.006
黄菊提取物分析方法研究
Analytical method for Huangju extract
刘伟毅 1李玲 2丁越 2王冰2
作者信息
- 1. 上海制皂有限公司，上海 200331
- 2. 上海中医药大学教学实验中心，上海 201203
- 折叠
摘要
Abstract
TLC method was used for qualitative identiifcation of huangju extract (Ghrysanthemum indicum L.,Scutellaria baicalensis). HPLC method was used to determine the contents ofbaicalin, the moisture content and insoluble residue in huangju extract. TLC method can qualitatively identify theGhrysanthemum indicum L., by which the spots were clear with good separation and without interference in the negative reference. Thebaicalin showed a good linearity in the measurement range of 1.862 ~ 186.195 µg·mL-1 (r=0.999 7). The average recovery was 102.08% with the RSD (n=9) was 1.57%.关键词
药皂/黄菊提取物/黄芩苷/薄层色谱法/高效液相色谱法Key words
medicated soap/Huangju extract/baicalin/TLC/HPLC分类
化学化工引用本文复制引用
刘伟毅,李玲,丁越,王冰..黄菊提取物分析方法研究[J].日用化学品科学,2016,39(11):21-25,5.
