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光扩散用单分散交联聚甲基丙烯酸甲酯微球的制备及其表征∗

仝红亮 杨明山 尹鹏伟 刘厚磊

合成材料老化与应用2016,Vol.45Issue(6):15-20,6.
合成材料老化与应用2016,Vol.45Issue(6):15-20,6.

光扩散用单分散交联聚甲基丙烯酸甲酯微球的制备及其表征∗

Preparation and Characterization of Monodisperse Cross-linked Poly (methyl methacrylate) Microspheres for Light Scattering

仝红亮 1杨明山 2尹鹏伟 1刘厚磊2

作者信息

  • 1. 北京石油化工学院材料科学与工程学院 特种弹性体复合材料北京市重点实验室,北京102617
  • 2. 北京化工大学材料科学与工程学院,北京100029
  • 折叠

摘要

Abstract

Monodisperse cross-linked poly ( methyl methacrylate ) microspheres were prepared by dispersion polymerization with methyl methacrylate as reactant,2,2-azobisizobutyronitrile ( AIBN) as initiator,ethanol-water as solvent, polyvinylpyrrolidone ( PVP ) as dispersing agent and ethylene glycol dimethacrylate as cross-linking agent. The influence of ratio of ethanol/water medium,the concentration of the monomer and the type of cross-linking agent on the PMMA particles were investigated. And the samples were analysed and characterized by Fourier transform infrared spectrometer,laser particle size analyzer,thermal gravimetric analysis,scanning elec-tron microscopy.

关键词

聚甲基丙烯酸甲酯(PMMA)/交联微球/光扩散

Key words

poly( methyl methacrylate) ( PMMA)/cross-linked microspheres/light scattering

分类

化学化工

引用本文复制引用

仝红亮,杨明山,尹鹏伟,刘厚磊..光扩散用单分散交联聚甲基丙烯酸甲酯微球的制备及其表征∗[J].合成材料老化与应用,2016,45(6):15-20,6.

基金项目

北京石油化工学院研究生创新项目(16033981001/030)资助 (16033981001/030)

合成材料老化与应用

OACSTPCD

1671-5381

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