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金属有机骨架材料UiO-66的制备及表征

刘强

云南化工2016,Vol.43Issue(6):1-7,7.
云南化工2016,Vol.43Issue(6):1-7,7.DOI:10.3969/j.issn.1004-275X.2016.06.001

金属有机骨架材料UiO-66的制备及表征

Preparation and Characterization of Metal-organic Framework of UiO-66 materials

刘强1

作者信息

  • 1. 四川大学化学工程学院,成都610065
  • 折叠

摘要

Abstract

UiO-66 was synthesized by solvothermal method,using zirconiumchlorideasmetal salt, terephthalic acid as organic ligand,DMF as organic solvent.The factors of metal salt,organic solvent,or-ganic ligand,crystallizing temperature and time were investigated,the optimal synthesis conditions were met-al salt to organic ligand ratio at 1 ,organic solvent to organic ligand ratio at 25 ,crystallizing temperature at 100℃,and crystallizing time at 25h.The UiO-66 synthesized under the optimal conditions has higher rela-tive crystallinity.

关键词

金属有机骨架/溶剂热法/UiO-66

Key words

metal-organic framework/solvothermal method/UiO-66/synthesis

分类

化学化工

引用本文复制引用

刘强..金属有机骨架材料UiO-66的制备及表征[J].云南化工,2016,43(6):1-7,7.

云南化工

1004-275X

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