云南化工2016,Vol.43Issue(6):1-7,7.DOI:10.3969/j.issn.1004-275X.2016.06.001
金属有机骨架材料UiO-66的制备及表征
Preparation and Characterization of Metal-organic Framework of UiO-66 materials
摘要
Abstract
UiO-66 was synthesized by solvothermal method,using zirconiumchlorideasmetal salt, terephthalic acid as organic ligand,DMF as organic solvent.The factors of metal salt,organic solvent,or-ganic ligand,crystallizing temperature and time were investigated,the optimal synthesis conditions were met-al salt to organic ligand ratio at 1 ,organic solvent to organic ligand ratio at 25 ,crystallizing temperature at 100℃,and crystallizing time at 25h.The UiO-66 synthesized under the optimal conditions has higher rela-tive crystallinity.关键词
金属有机骨架/溶剂热法/UiO-66Key words
metal-organic framework/solvothermal method/UiO-66/synthesis分类
化学化工引用本文复制引用
刘强..金属有机骨架材料UiO-66的制备及表征[J].云南化工,2016,43(6):1-7,7.