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β2-SiW11/TiO2光催化剂的制备及光催化性能

马荣华 丁玲玉 李晓宇

印染助剂Issue(12):7-10,18,5.
印染助剂Issue(12):7-10,18,5.

β2-SiW11/TiO2光催化剂的制备及光催化性能

Preparation and photocatalytic performance of photocatalyst β2-SiW11/TiO2

马荣华 1丁玲玉 1李晓宇1

作者信息

  • 1. 齐齐哈尔大学化学与化学工程学院,黑龙江齐齐哈尔 161006
  • 折叠

摘要

Abstract

The composite photocatalyst β2-SiW11/TiO2 was prepared by impregnating silicotungstate on ti⁃tanium dioxide by impregnation method, β2-K8SiW11O39·xH2O as active component. Then catalyst β2-SiW11/TiO2 were characterized by infrared spectroscopy (IR), UV spectroscopy, thermal gravimetric (TG), X-ray photoelec⁃tron spectroscopy (XPS), X-ray diffraction (XRD) and scanning electron microscopy (SEM). Meanwhile, the pho⁃tocatalytic activity of the catalyst was assessed using the photocatalytic degradation of methylene blue, a mod⁃el pol utant, as a probe. The influences of the β2-SiW11/TiO2 dosage and the solution pH on the catalyst activity were examined. The results showed that compared with TiO2 and β2-K8SiW11O39·xH2O, β2-SiW11/TiO2 had the advantage, which played a synergistic effect. The degradation rate of methylene blue was 82.53%.

关键词

杂多硅钨酸盐/二氧化钛/光催化性能/亚甲基蓝

Key words

heteropoly silicotungstate/titanium dioxide/photocatalytic performance/methylene blue

分类

资源环境

引用本文复制引用

马荣华,丁玲玉,李晓宇..β2-SiW11/TiO2光催化剂的制备及光催化性能[J].印染助剂,2016,(12):7-10,18,5.

基金项目

黑龙江省自然科学基金(B2007-15);黑龙江省教育厅基金(12531760);齐齐哈尔大学研究生创新基金 ()

印染助剂

OA北大核心CSTPCD

1004-0439

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