广西科学院学报2016,Vol.32Issue(4):278-281,4.DOI:10.13657/j.cnki.gxkxyxb.20161128.001
三七花颗粒的质量控制方法
Study on the Quality Control Method of Sanchi Gran-uLe
摘要
Abstract
[Objective]To perfect the quality control standard of sanchi granuLe.[Methods]The TLC method was used to identify the sanchi granuLe and the HPLC method was used for the determination of ginsenoside Rb3 in it.[Results]Each of the sanchi,sanchi granuLe and gin-senoside Rb3 had a similar fluorescent spot which performed the same colour and Rf in the TLC.The calibration curve of ginsenoside Rb3 showed a good linearity within 0.505~5.050μg,r=0.999 9.The average recovery was 101.25%,RSD was 0.54%(n=6).[Conclusion]The method was simple and accurate,it could be used for the quality control of Sanchi Gran-uLe.关键词
高效液相色谱/薄层色谱/三七花颗粒/人参皂苷 Rb3Key words
HPLC/TLC/sanchi granuLe/ginsenoside Rb3分类
医药卫生引用本文复制引用
冯军,刘布鸣..三七花颗粒的质量控制方法[J].广西科学院学报,2016,32(4):278-281,4.基金项目
广西中药质量标准研究重点实验室系统性研究课题(桂中重系201310)和广西科学研究与技术开发项目(重大专项计划,桂科重14124002-11)资助。 (桂中重系201310)