实验科学与技术2016，Vol.14Issue(6)：177-179,195,4.DOI:10.3969/j.issn.1672-4550.2016.06.046
大学化学“薄层色谱实验”的改进
The Improvement of University Chemistry of TLC Experiment
刘璐 1田鹏 1丁克廉 1傅旭阳1
作者信息
- 1. 西北农林科技大学 理学院，陕西 杨凌 712100
- 折叠
摘要
Abstract
In order to find a low toxicity and easy operation method of thin layer chromatography experiment,traditional method of membrane separation for mixtures of anisaldehyde and vanillin was improved,this paper investigated the optimization design of the sol-vent,developing agent .absolute ethanol was selected as the solvent.At the same time,petroleum ether and ethyl acetate (the ratio was 7∶3)were selected as developing solvent .Acidic potassium permanganate was selected as chromomeric agent to replace the toxicity of higher benzene and 2,4 dinitrobenzene hydrazine hydrochloride solvent.The steps,cost and time of experiment was reduced.The new scheme reduced harm of people health and pollute the environment.The method could separate anisaldehyde and vanillin from mixtures .关键词
茴香醛/香草醛/薄层色谱/实验方法Key words
anisaldehyde/vanillin/thin layer chromatography/method of experiment分类
数理科学引用本文复制引用
刘璐,田鹏,丁克廉,傅旭阳..大学化学“薄层色谱实验”的改进[J].实验科学与技术,2016,14(6):177-179,195,4.
