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端环氧硅油及其嵌段亲水硅油的制备及应用性能

袁洁 贺江平 颜怀谦 冯娜

印染助剂2017,Vol.34Issue(1):27-31,5.
印染助剂2017,Vol.34Issue(1):27-31,5.

端环氧硅油及其嵌段亲水硅油的制备及应用性能

Preparation and application of end epoxy silicone oil and its block hydrophilic silicone oil

袁洁 1贺江平 1颜怀谦 1冯娜1

作者信息

  • 1. 西安工程大学纺织与材料学院,陕西西安 710048
  • 折叠

摘要

Abstract

The synthesis process of end epoxy silicone oil was as fol ows: the mass ratio of D4 and epoxy was 12.79∶1, then 0.08% tetramethyl ammonium hydroxide was added, vacuumed at 70 ℃ for 20 min, the temperature was raised to 110 ℃ for 4 h, heating to 140 ℃ for 1 h, and final y cooling to 40 ℃, the end epoxy silicone oil with relative molecular weight of 5 000 was prepared, which was modified by hydrophilic modifica⁃tion ED900. The hand feeling of finished cotton fabrics was 4~5 level, stiffness was 1.45 cm, the static fric⁃tion coefficient was 0.311, the strength increased to 320 N, the whiteness decreased slightly, the hydrophilic reached 8 s, and the wrinkle recovery angle increased by about 20°.

关键词

环氧封端剂/聚醚胺/端环氧硅油/亲水改性

Key words

epoxy sealing head agent/polyether amino/end epoxy silicone oil/hydrophilic modification

分类

化学化工

引用本文复制引用

袁洁,贺江平,颜怀谦,冯娜..端环氧硅油及其嵌段亲水硅油的制备及应用性能[J].印染助剂,2017,34(1):27-31,5.

印染助剂

OA北大核心CSTPCD

1004-0439

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