中国中医药信息杂志2017，Vol.24Issue(3)：78-81,4.DOI:10.3969/j.issn.1005-5304.2017.03.019
三元乳癖消凝胶膏质量标准研究
Study on Quality Standard of Sanyuan Rupixiao Gel Paste
摘要
Abstract
Objective To establish the quality standard for Sanyuan Rupixiao Gel Paste. Methods Sparganii Rhizoma, Gleditsiae Sinensis Fructus, Cyperi Rhizoma and Impatientis Semen were identified by TLC method. The content of tetrahydropalmatine was determined by HPLC. Waters symmetry column was used with the mobile phase of acetonitrile-0.1% phosphatic acid in a gradient manner (pH was adjusted to 6.4 by triethylamine) (55:45) at the detection wavelength of 280 nm. The flow rate was 1.0 mL/min at the column temperature of 30 ℃. Results The spots in TLC were clear without any interference;tetrahydropalmatine showed a good linear relation in the range of 0.092–1.84 µg;the average recovery was 100.15%with RSD of 1.58%(n=6). Conclusion The method is simple and accurate with high reproducibility, which can be used for the quality control of Sanyuan Rupixiao Gel Paste.关键词
三元乳癖消凝胶膏/急性子/质量标准/薄层色谱法/高效液相色谱法Key words
Sanyuan Rupixiao Gel Paste/Impatientis Semen/quality standard/TLC/HPLC分类
医药卫生引用本文复制引用
王卓,程玉钏,李媛媛,郭丁丁,倪艳,郝旭亮,孔朋,姚姣妮,梁泽..三元乳癖消凝胶膏质量标准研究[J].中国中医药信息杂志,2017,24(3):78-81,4.基金项目
山西省科技重大专项研究项目 （）
