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PAN预氧纤维径向结构的光密度法研究

钟珊 徐帆 雷帅 武帅 徐樑华

材料工程2017,Vol.45Issue(2):65-71,7.
材料工程2017,Vol.45Issue(2):65-71,7.DOI:10.11868/j.issn.1001-4381.2015.001275

PAN预氧纤维径向结构的光密度法研究

Optical Density Method of Radial Structure of PAN-based Pre-oxidized Fibers

钟珊 1徐帆 1雷帅 1武帅 1徐樑华1

作者信息

  • 1. 北京化工大学碳纤维及功能高分子教育部重点实验室 ,北京100029
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摘要

Abstract

According to the radial distribution characteristics of PAN pre-oxidized fiber ,the optical density method which can quantitatively characterize the radial structure of pre-oxidized PAN fiber is established ,taking advantage of the light-absorbing of PAN pre-oxidized structure .The results show that when the sample's width is 400 nm and the light intensity is 800 lx ,the optical density method characterize the radial distribution characteristics of PAN pre-oxidized fibers the most effectively and accurately .Compared with the traditional skin-core structure characterization method ,this method not only expresses the pre-oxidized degree in the same domain under different pre-oxidation processes , but also obtains the radial distribution of pre-oxidized degree .Applying this method to the process re-search of pre-oxidized PAN fiber ,the results show that this method can reveal a correlation between the process and structure ,indicating the optical density method as a new method for characterization of PAN pre-oxidized fiber can play an active role in the study of pre-oxidized PAN radial structure .

关键词

PAN纤维/光密度法/径向结构/预氧化程度

Key words

PAN fiber/optical density method/radial structure/pre-oxidation

分类

化学化工

引用本文复制引用

钟珊,徐帆,雷帅,武帅,徐樑华..PAN预氧纤维径向结构的光密度法研究[J].材料工程,2017,45(2):65-71,7.

基金项目

国家973项目(2011CB605602) (2011CB605602)

材料工程

OA北大核心CSCDCSTPCD

1001-4381

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