波谱学杂志2017，Vol.34Issue(1)：35-42,8.DOI:10.11938/cjmr20170105
雷酚内酯的波谱学数据与结构确证
Spectral Analysis and Structural Elucidation of Triptophnolide
摘要
Abstract
Ultraviolet (UV) spectrum, infrared (IR) spectrum, mass (MS) spectra and nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT, 1H-1H COSY, NOE, 1H-13C HSQC and 1H-13C HMBC) of Triptophnolide were collected and interpreted. All 1H and 13C NMR signals were assigned. Base on the data, the structure of reference standard Triptophnolide was determined.关键词
核磁共振(NMR)/归属/化学位移/雷酚内酯/结构确证Key words
nuclear magnetic resonance (NMR)/assignment/chemical shift/Triptophnolide/structural elucidation分类
数理科学引用本文复制引用
王菲菲,张聿梅,何轶,戴忠,马双成,刘斌..雷酚内酯的波谱学数据与结构确证[J].波谱学杂志,2017,34(1):35-42,8.基金项目
十二五"重大新药创制"专项课题"中药质量安全检测及风险控制平台"资助项目(2014ZX09304307-002). （2014ZX09304307-002）
