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响应面法优化白花菜中黄酮类化合物的提取研究

王菲 山显彤 张家境 王战勇

辽宁石油化工大学学报2017,Vol.37Issue(1):18-23,6.
辽宁石油化工大学学报2017,Vol.37Issue(1):18-23,6.DOI:10.3969/j.issn.1672-6952.2017.01.004

响应面法优化白花菜中黄酮类化合物的提取研究

Optimization on the Extraction Conditions of Flavonoids from Cauliflower Using Response Surface Methodology

王菲 1山显彤 1张家境 1王战勇1

作者信息

  • 1. 辽宁石油化工大学化学化工与环境学部,辽宁抚顺113001
  • 折叠

摘要

Abstract

The flavonoids was extracted from cauliflower by using ultrasonic-assisted solvent and the response surface methodology was used to optimize the extraction conditions .Firstly , the effects of different extraction factors (ethanol concentration ,liquid-material ratio ,ultrasonic power ,ultrasonic time ,bath temperature ,bath time and extraction times) on flavonoids yield were studied .And then ,Box-Behnken response surface optimization test was carried on the basic of singer factor test result .The optimal conditions were as follows :65% ethanol ,liquid-solid ratio 32:1 mL/g ,ultrasonic power 30 W ,ultrasonic time 5 min ,bath temperature 50 ℃ ,bath time 40 min ,and extraction time 1 .Under this optimum conditions , the actual yield of flavonoids was 1.9745 mg/g ,and it was very close to the prediction value .

关键词

白花菜/黄酮类化合物/提取/响应面法

Key words

Cauliflower/Flavonoids/Extraction/Response surface methodology

分类

轻工纺织

引用本文复制引用

王菲,山显彤,张家境,王战勇..响应面法优化白花菜中黄酮类化合物的提取研究[J].辽宁石油化工大学学报,2017,37(1):18-23,6.

基金项目

辽宁省高等学校杰出青年学者成长计划项目(LJQ2014040). (LJQ2014040)

辽宁石油化工大学学报

1672-6952

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