天然产物研究与开发2017，Vol.29Issue(2)：245-248,244,5.DOI:10.16333/j.1001-6880.2017.2.011
头序瓜馥木化学成分研究
Chemical Constituents from Fissistigma retusum
摘要
Abstract
To study the chemical constituents from stems and leaves of Fissistigma retusum.The chemical constituents from F.retusum were separated and purified by silica gel,ODS,Sephadex LH-20 gel column chromatographies,and preparative HPLC.Their structures were identified by physicochemical properties,spectroscopic analysis,as well as comparisons with the literature data.As a result,12 compounds were isolated from 95％ ethanol extract from F.retusum,and identified as protocatechuic acid ethyl ester (1),(S)-methoxy-(3,5-dimethoxy-4-hydroxyphenyl) ethanediol (2),2-cis4-trans-abscisicacid (3),kaempferol-3-O-a-L-arabinopyranoside (4),naringenin (5),aromadendrin (6),eriodictyol (7),(2R,3S)-5,7,3'-tri-methoxy-epicatechin (8),5,6,8-tri-methoxy-7-hydro-xylflavonone (9),syringaresinol (10),epiyangambin (11) and seartemin (12).Compounds 1-12 were isolated from the genus Fissistigma for the first time.关键词
头序瓜馥木/化学成分/酚酸/萜类/黄酮/木脂素Key words
Fissistigma retusum/chemical constituents/phenolic acids/terpenes/flavonoids/lignans分类
化学化工引用本文复制引用
张航旗,周戚,付艳辉,陈光英,杨娜英..头序瓜馥木化学成分研究[J].天然产物研究与开发,2017,29(2):245-248,244,5.基金项目
973计划前期研究专项(2014CB560714) （2014CB560714）
海南省自然基金科技创新团队(2016CXTD007) （2016CXTD007）
